HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21506092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 21506098 | HCID 21506098 | — |
| Product | HCID 21506092 | HCID 21506092 | — |
Reaction Steps
A mixture of 3 -amino-4-anilino-5-sulphamyl-benzoic acid (2 g), benzyl bromide (3 g), and ethanol (50 ml 99.9%) was refluxed for 8 hours. After cooling, the ethyl-4-anilino-3-benzylamino-5-sulphamyl-benzoate crystallized and was collected by suction. After recrystallization from ethanol the melting point was 160°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-233464decfd14948b5fe9efcf4bc56e4 |
| Source note | uspto-grants-1976_10 |