HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21505996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Amino-4-phenoxy-5-sulfamoylbenzoic acid | HCID 119927 | — |
| Solvent | 1-Pentanol | HCID 6276 | — |
| Product | HCID 21505996 | HCID 21505996 | — |
Reaction Steps
A mixture of 3-amino-4-phenoxy-5-sulphamyl-benzoic acid (6 g), n-pentanol (60 ml), and conc. sulphuric acid (0.5 ml) was refluxed for 24 hours. After cooling, the precipitated n-pentyl 3-pentylamino-4-phenoxy-5-sulphamyl-benzoate was isolated by filtration and recrystallized from n-pentanol. After drying in vacuo, the compound was obtained with a melting point of 138°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a7494207e4014e0195975bdb5620cb0e |
| Source note | uspto-grants-1976_10 |