Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 4-Chloro-3-nitro-5-sulphamoylbenzoic acid | HCID 89893 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21506110 | HCID 21506110 | — |
Reaction Steps
A mixture of 4-chloro-3-nitro-5-sulphamyl-benzoic acid (8.4 g), n-butylamine (8.7 g), and water (25 ml) was stirred at 90° C for 1.5 hours. After cooling, the pH was adjusted to pH 2, and the precipitated 4-butylamino-3-nitro-5-sulphamyl-benzoic acid was collected by filtration. After several recrystallizations from aqueous methanol the melting point was 192.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03985777 |
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| Source dataset | uspto-grants-1976_10 |
|---|
| ORD ID | ord-02b362a9135c42a289e261d912183610 |
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| Source note | uspto-grants-1976_10 |
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