HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 21506104 | HCID 21506104 | — |
| Product | Ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate | HCID 21506051 | — |
Reaction Steps
A mixture of 3-amino-5-dimethylsulphamyl-4-phenoxy-benzoic acid (1.68 g), benzyl bromide (2 g), and ethanol (15 ml) was refluxed for 5 hours. After cooling, the precipitated ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate was isolated and recrystallized from ethanol. After drying in vacuo, the compound was obtained with a melting point of 154°-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-9cb03739ac4a4a09b85ed2d5b0d97cbf |
| Source note | uspto-grants-1976_10 |