HRID1287807

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID702

Ethanol

C2H6O

HCID7498

alpha-Bromotoluene

C7H7Br

结构：CN(C)S(=O)(=O)c1cc(C(=O)O)cc(N)c1Oc1ccccc1

HCID21506104

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1cc(NCc2ccccc2)c(Oc2ccccc2)c(S(=O)(=O)N(C)C)c1

HCID21506051

未命名化合物

PROCEDURE

实验过程

A mixture of 3-amino-5-dimethylsulphamyl-4-phenoxy-benzoic acid (1.68 g), benzyl bromide (2 g), and ethanol (15 ml) was refluxed for 5 hours. After cooling, the precipitated ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate was isolated and recrystallized from ethanol. After drying in vacuo, the compound was obtained with a melting point of 154°-155° C.

WORKUP

后处理

temperaturewas refluxed for 5 hours
temperatureAfter cooling