HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 68141669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 21506585 | HCID 21506585 | — |
| Reactant | HCID 21506588 | HCID 21506588 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 68141669 | HCID 68141669 | — |
Reaction Steps
A sample of 1H, 3H-oxazolo[3,4-a]perimidine-3-one is dissolved in dimethoxyethane and is treated with excess conc. ammonia. The separated solid, (2-perimidyl)methyl carbamate, is filtered, dissolved in ethanol and treated with hydrochloric acid to give the acid addition salt, (2-perimidyl)methyl carbamate hydrochloride, m.p. 240° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985880 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-d48920d9dcda4bfc812e0772d8a71976 |
| Source note | uspto-grants-1976_10 |