HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroacetate → HCID 21506545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroacetate | HCID 7295 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(4-Chlorophenoxy)phenol | HCID 12346120 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 21506545 | HCID 21506545 | 92.2% |
Reaction Steps
6.6 g (30 millimols) of 4-(4'-chlorophenoxy)phenol, 4.14 g (30 millimols) of potassium carbonate, 60 ml. of methyl ethyl ketone and 5.0 g (45 millimols) of methyl chloroacetate were treated in the same way as in Referential Example 2 to afford 8.1 g of oily methyl 4-(4'-chlorophenoxy)phenoxyacetate in a yield of 92%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985875 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-b68933ac111945b089d698ec93d83a2d |
| Source note | uspto-grants-1976_10 |