HRID1287904

反应详情

EQUATION

反应方程式

HRID 1287904 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 1.02 g. of 1,3-dihydrospiro[isobenzofuran-1,4'-piperidine]-3-one, 1.0 g. of sodium bicarbonate, 10 ml. of chloroform, and 0.60 g. of allyl bromide is stirred at room temperature for 24 hours and filtered. The filtrate is washed with water, dried over potassium caarbonate, and concentrated to an oily solid.

WORKUP

后处理

  1. additionA mixture of 1.02 g
  2. filtrationfiltered
  3. washThe filtrate is washed with water
  4. dry with materialdried over potassium caarbonate
  5. concentrationconcentrated to an oily solid