HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54344879, compound → HCID 53769299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54344879 | HCID 54344879 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53769299 | HCID 53769299 | — |
Reaction Steps
The 2,6 diphenyl-4-(p-ethoxyphenyl) pyridine is then dissolved in glacial acetic acid (20ml) to which 0.2g of Adam's catalyst is added. The compound is then hydrogenated at 3 atm with shaking for 4-5 hours. The catalyst and solvent were removed from the reaction mixture leaving 2,6-dicyclohexyl-4-(p-ethoxyphenyl) pyridine m.p. 106°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03986140 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a0dfa531dfdb4410ab1894f482448ec3 |
| Source note | uspto-grants-1976_10 |