HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 19917663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 21503370 | HCID 21503370 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19917663 | HCID 19917663 | 98.3% |
Reaction Steps
15.9 g of 2-ethoxycarbonylmethyl-quinuclidine were reduced with lithium aluminium hydride in the presence of ether under reflux to give 12.3 g of 2-hydroxyethylquinuclidine, m.p. 62°-64° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987042 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-faa271a377844fd8aeff5400a4719516 |
| Source note | uspto-grants-1976_10 |