HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-2-nitro-1H-imidazole-5-carboxaldehyde → HCID 53759317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-2-nitro-1H-imidazole-5-carboxaldehyde | HCID 100390 | — |
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53759317 | HCID 53759317 | — |
Reaction Steps
A solution of 1.42 g. of thiosemicarbazide in water is added to a solution of 1.8 g. of 1-methyl-2-nitro-5-imidazolecarboxaldehyde in methanol. The solid which precipitates is recovered on the filter. Yield: 2.2 g., m.p. 282°-287° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987053 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-d302eb8bbeb34008984672f536bb57fe |
| Source note | uspto-grants-1976_10 |