Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetohydrazide | HCID 14039 | — |
| Reactant | HCID 19865807 | HCID 19865807 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21489308 | HCID 21489308 | — |
Reaction Steps
In the manner given in Example 2, 6,9-dichloro-1,3-dihydro-5-(p-isopropylphenyl)-2H-1,4-benzodiazepine-2-thione is heated in ethanol with acetic acid hydrazide and the resulting product heated to 250° C. to give 7,10-dichloro-1-methyl-6-(p-isopropylphenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03987052 |
|---|
| Source dataset | uspto-grants-1976_10 |
|---|
| ORD ID | ord-93e960a7975a4d9c9a384a828026f222 |
|---|
| Source note | uspto-grants-1976_10 |
|---|
