Hydrochloric Acid → HCID 21503498, compound

HRID 1288110Notes

Reaction equation

HRID 1288110 reaction equation
[ClH:1].C([N:5]1[CH2:20][CH2:19][CH2:18][C:8]2=[N:9][C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][C:15]=3[C:16]([Cl:17])=[C:7]2[CH2:6]1)(=O)C.Cl.C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl>>[ClH:17].[ClH:1].[Cl:17][C:16]1[C:15]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[N:9]=[C:8]2[CH2:18][CH2:19][CH2:20][NH:5][CH2:6][C:7]=12

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 149026Tetrafluoro-m-phenylenediamine dihydrochlorideHCID 21503575HCID 21503575, compound

Product 1

HCID 21503498HCID 21503498, compound

Procedure

11-Chloro-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline dihydrochloride was prepared by hydrolysis of 2-acetyl-11-chloro-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline hydrochloride with 2 N hydrochloric acid. Yield of the dihydrochloride: 11% of theory; m.p. 260° C. (decomp.).

Sources & evidence

ORD record
ord-73ed9366eb184bd6a939a818d02fa06c
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

Loading…