HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | HCID 178524303 | HCID 178524303 | — |
| Product | HCID 178478867 | HCID 178478867 | — |
Reaction Steps
11-Hydroxy-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline dihydrochloride was prepared by hydrolysis of 11-hydroxy-2-phenoxycarbonyl-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline with concentrated hydrochloric acid. Yield of the dihydrochloride: 65% of theory; m.p. 289° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-fa515954e0724f98bf55d4b3b6b3618f |
| Source note | uspto-grants-1976_10 |