HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → 3-(p-Chloro-benzoyl)-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | 11-methyl-2,3,4,5-tetrahydro-1H-azepino[4,5-b]quinoline | HCID 3043999 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3-(p-Chloro-benzoyl)-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline | HCID 21503611 | 65% |
Reaction Steps
3-(p-Chloro-benzoyl)-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline was prepared from 1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline and 4-chloro-benzoyl chloride in pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-689b519ae90946a6bba4eb359b25e317 |
| Source note | uspto-grants-1976_10 |