Hydrogen Peroxide → HCID 21503637, compound

HRID 1288152Notes

Reaction equation

[C:1]([N:4]1[CH2:18][CH2:17][C:16]2[C:7](=[N:8][C:9]3[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=3[C:15]=2[CH3:19])[CH2:6][CH2:5]1)(=[O:3])[CH3:2].[OH:20]O>>[C:1]([N:4]1[CH2:18][CH2:17][C:16]2[C:7](=[N+:8]([O-:20])[C:9]3[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=3[C:15]=2[CH3:19])[CH2:6][CH2:5]1)(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 215035013-acetyl-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline

Product 1

HCID 21503637HCID 21503637, compoundYield 83.5%

Procedure

3-Acetyl-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline 6-oxide was prepared analogous to Example 111 from 3-acetyl-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline and hydrogen peroxide.

Sources & evidence

ORD record: ord-2592fcf140b64742b85b5e872ce8b453
Source dataset: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03987047

Reaction notes

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