Hydrogen Peroxide → HCID 54429096, compound

HRID 1288153Notes

Reaction equation

[CH2:1]([O:3][C:4]([N:6]1[CH2:21][CH2:20][CH2:19][C:9]2=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]([CH3:18])=[C:8]2[CH2:7]1)=[O:5])[CH3:2].[OH:22]O>>[CH2:1]([O:3][C:4]([N:6]1[CH2:21][CH2:20][CH2:19][C:9]2=[N+:10]([O-:22])[C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]([CH3:18])=[C:8]2[CH2:7]1)=[O:5])[CH3:2]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 53845549HCID 53845549, compound

Product 1

HCID 54429096HCID 54429096, compoundYield 60%

Procedure

2,3,4,5-Tetrahydro-11-methyl-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester 6-oxide was prepared analogous to Example 111 from 2,3,4,5-tetrahydro-11-methyl-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester and hydrogen peroxide.

Sources & evidence

ORD record: ord-830fca965c5d4c78ac32653cb8ea6b69
Source dataset: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03987047

Reaction notes

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