HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 53813451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 53994340 | HCID 53994340 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 53813451 | HCID 53813451 | 95% |
Reaction Steps
9-Amino-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester was prepared from 9-nitro-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester by reduction with nascent hydrogen, generated in situ by concentrated hydrochloric acid and tin(II)chloride, at a temperature of 60°-80° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-8424d84b530d416bb11331649fcb0baf |
| Source note | uspto-grants-1976_10 |