HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 53744550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 53875304 | HCID 53875304 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53744550 | HCID 53744550 | — |
Reaction Steps
2 gm (6.65 millimols) of 5-hydroxy-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester were converted into the sodium salt in 50 ml of absolute tetrahydrofuran with 0.32 gm (7 millimols) of 50% sodium hydride, and the salt was methylated with 0.43 ml (7 millimols) of methyl iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-dcf75a0daf3e4a969ea902ba14092028 |
| Source note | uspto-grants-1976_10 |