Hydrochloric Acid → HCID 68140001, compound

HRID 1288181Notes

Reaction equation

HRID 1288181 reaction equation
C([O:3][C:4](=[O:22])[CH2:5][N:6]1[CH2:20][CH2:19][C:18]2[C:9](=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]=2[CH3:21])[CH2:8][CH2:7]1)C.[ClH:23]>>[ClH:23].[ClH:23].[CH3:21][C:17]1[C:16]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[N:10]=[C:9]2[CH2:8][CH2:7][N:6]([CH2:5][C:4]([OH:22])=[O:3])[CH2:20][CH2:19][C:18]=12

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 54143292HCID 54143292, compound

Product 1

HCID 68140001HCID 68140001, compoundYield 72%

Procedure

2-[1,2,4,5-Tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline-3-yl]acetic acid dihydrochloride was prepared by hydrolysis of 2-[1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline-3-yl]acetic acid ethyl ester in 2 N hydrochloric acid at the boiling point.

Sources & evidence

ORD record
ord-b907a3687c2641f0afcbf4c3049980b6
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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