HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21503398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 11-Methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester | HCID 53801409 | — |
| Product | HCID 21503398 | HCID 21503398 | 7% |
Reaction Steps
11-methoxy-1,2,4,5-tetrahydro-3H-azepino[4,5-b]quinoline was prepared from 11-methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b] quinoline-carboxylic acid ethyl ester by hydrolysis with semiconcentrated hydrochloric acid. Yield: 7% of theory; m.p. 112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-9972402c51914d2f8bf48c32680d999e |
| Source note | uspto-grants-1976_10 |