Hydrochloric Acid → HCID 21503398, compound

HRID 1288191Notes

Reaction equation

HRID 1288191 reaction equation
C(OC([N:6]1[CH2:20][CH2:19][C:18]2[C:9](=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]=2[O:21][CH3:22])[CH2:8][CH2:7]1)=O)C.Cl>>[CH3:22][O:21][C:17]1[C:16]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[N:10]=[C:9]2[CH2:8][CH2:7][NH:6][CH2:20][CH2:19][C:18]=12

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 5380140911-Methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester

Product 1

HCID 21503398HCID 21503398, compoundYield 7%

Procedure

11-methoxy-1,2,4,5-tetrahydro-3H-azepino[4,5-b]quinoline was prepared from 11-methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b] quinoline-carboxylic acid ethyl ester by hydrolysis with semiconcentrated hydrochloric acid. Yield: 7% of theory; m.p. 112° C.

Sources & evidence

ORD record
ord-9972402c51914d2f8bf48c32680d999e
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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