HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 178473335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 178515156 | HCID 178515156 | — |
| Product | HCID 178473335 | HCID 178473335 | 9% |
Reaction Steps
11-Hydroxy-2,3,4,5-tetrahydro-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester was prepared from 2-benzyl-11-hydroxy-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline and ethyl chloroformate analogous to Example 208. Yield: 9% of theory; m.p. 285° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-e3bd3fc398714bf3a1e5b44f957f50d3 |
| Source note | uspto-grants-1976_10 |