HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 53684965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 21503414 | HCID 21503414 | — |
| Product | HCID 53684965 | HCID 53684965 | 79% |
Reaction Steps
8,11-Dimethyl-1,2,4,5-tetrahydro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester was prepared from 8,11-dimethyl-1,2,4,5-tetrahydro-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 155. Yield: 79% of theory; m.p. 121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-c5cc336f6a9740ad8c2a9dd1194e2f78 |
| Source note | uspto-grants-1976_10 |