HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54274069, compound → HCID 21503565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54274069 | HCID 54274069 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21503565 | HCID 21503565 | 36% |
Reaction Steps
3-Thiocarbamoyl-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline was prepared by hydrolysis of 3-(benzamido-thiocarbonyl)-1,2,4,5-tetrahydro-11-methyl-azepino[4,5-b]quinoline (m.p. 175° C) in 2 N sodium hydroxide at room temperature. Yield: 36 % of theory; m.p. 218° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a46c1d9e48a24f69887fc62543eebd2c |
| Source note | uspto-grants-1976_10 |