Methyl iodide → HCID 21504220, compound

HRID 1288240Notes

Reaction equation

HRID 1288240 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([NH2:11])=[S:10])=[CH:4][CH:3]=1.[CH3:12][I:13]>CC(C)=O>[IH:13].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][C:9](=[NH:11])[S:10][CH3:12])=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 27348272-(4-chlorophenyl)ethanethioamide

Product 1

HCID 21504220HCID 21504220, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A solution of 4-chlorophenyl(thioacetamide) (14.8 g.) and methyl iodide (32 g.) in acetone (40 ml.) was heated to reflux for 20 minutes. The mixture was cooled and filtered to give pure methyl 4-chlorophenyl(thioacetimidate) hydriodide, m.p. 172°-174°.

Workup

  1. temperatureto reflux for 20 minutes
  2. temperatureThe mixture was cooled
  3. filtrationfiltered

Sources & evidence

ORD record
ord-551e63de6d3a4c639e3f62e570ad9240
Source dataset
uspto-grants-1976_10
Patent number
US03987158

Reaction notes

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