HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21504220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-(4-Chlorophenyl)ethanethioamide | HCID 2734827 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21504220 | HCID 21504220 | — |
Reaction Steps
A solution of 4-chlorophenyl(thioacetamide) (14.8 g.) and methyl iodide (32 g.) in acetone (40 ml.) was heated to reflux for 20 minutes. The mixture was cooled and filtered to give pure methyl 4-chlorophenyl(thioacetimidate) hydriodide, m.p. 172°-174°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987158 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-551e63de6d3a4c639e3f62e570ad9240 |
| Source note | uspto-grants-1976_10 |