Methyl iodide → HCID 86734090, compound

HRID 1288243Notes

Reaction equation

HRID 1288243 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][C:9]([NH2:11])=[S:10])[CH:5]=[CH:6][CH:7]=1.[CH3:12][I:13]>CC(C)=O>[IH:13].[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][C:9](=[NH:11])[S:10][CH3:12])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 21504242(3-Methylphenyl)ethanethioamide

Product 1

HCID 86734090HCID 86734090, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A solution of 3-methylphenyl(thioacetamide) (4.9 g.) and methyl iodide (12.6 g.) in acetone (15 ml.) was heated to reflux for 20 minutes. The mixture was cooled and filtered to give pure methyl 3-methylphenyl(thioacetimidate) hydriodide, m.p. 142°-144°.

Workup

  1. temperatureto reflux for 20 minutes
  2. temperatureThe mixture was cooled
  3. filtrationfiltered

Sources & evidence

ORD record
ord-2c8adfebda864e26b97a632d83530a9a
Source dataset
uspto-grants-1976_10
Patent number
US03987158

Reaction notes

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