HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86734090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | (3-Methylphenyl)ethanethioamide | HCID 21504242 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86734090 | HCID 86734090 | — |
Reaction Steps
A solution of 3-methylphenyl(thioacetamide) (4.9 g.) and methyl iodide (12.6 g.) in acetone (15 ml.) was heated to reflux for 20 minutes. The mixture was cooled and filtered to give pure methyl 3-methylphenyl(thioacetimidate) hydriodide, m.p. 142°-144°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987158 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-2c8adfebda864e26b97a632d83530a9a |
| Source note | uspto-grants-1976_10 |