HRID1288310

反应详情

EQUATION

反应方程式

HRID 1288310 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 7.9 g. of 4-acetylamino-3,5-bis-trifluoromethylnitrobenzene in 200 ml. of ethanol is hydrogenated under 40 lbs. of hydrogen pressure with 1 g. of 5% palladium on charcoal catalyst. When the calculated amount of hydrogen is consumed, the solution is filtered and concentrated in vacuo to give 4-acetylamino-3,5-bis-trifluoromethylaniline.

WORKUP

后处理

  1. customWhen the calculated amount of hydrogen is consumed
  2. filtrationthe solution is filtered
  3. concentrationconcentrated in vacuo