HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylamino-3,5-bis-trifluoromethylnitrobenzene → HCID 21482728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylamino-3,5-bis-trifluoromethylnitrobenzene | HCID 21482725 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21482728 | HCID 21482728 | — |
Reaction Steps
A solution of 7.9 g. of 4-acetylamino-3,5-bis-trifluoromethylnitrobenzene in 200 ml. of ethanol is hydrogenated under 40 lbs. of hydrogen pressure with 1 g. of 5% palladium on charcoal catalyst. When the calculated amount of hydrogen is consumed, the solution is filtered and concentrated in vacuo to give 4-acetylamino-3,5-bis-trifluoromethylaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987199 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-c4128c22553d49c8ba083c757ab5fca2 |
| Source note | uspto-grants-1976_10 |