Boric Acid → Trilithium borate

HRID 1288404Notes

Reaction equation

HRID 1288404 reaction equation
OC(CCCCCC)CCCCCCCCCCC(O)=O.[B:22]([OH:25])([OH:24])[OH:23].O.[OH-].[Li+:28]>>[B:22]([OH:25])([O-:24])[O-:23].[Li+:28].[Li+:28].[B:22]([O-:25])([O-:24])[O-:23].[Li+:28].[Li+:28].[Li+:28]

Participants

5

Reactant 3

HCID 7628Boric AcidHCID 778912-Hydroxystearic acidHCID 168937Lithium hydroxide, monohydrate

Product 2

HCID 13743157Trilithium borateHCID 86734101HCID 86734101, compound

Procedure

Two additional 5 kg batches of grease were prepared. In each case the same proportion of 12-hydroxy-stearic acid and boric acid as in the grease A but increasing the amount of lithium hydroxide monohydrate so as to form dilithium borate (Grease 2) and trilithium borate (Grease 3) instead of monolithium borate (Grease A).

Workup

  1. customTwo additional 5 kg batches of grease were prepared

Sources & evidence

ORD record
ord-71c6a283f2294a79bf46c578519cdd3b
Source dataset
uspto-grants-1976_10
Patent number
US03988248

Reaction notes

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