HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-nitrobenzoic acid → 4-Chlorophenyl 2-chloro-4-nitrophenyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-nitrobenzoic acid | HCID 7448 | — |
| Reactant | Chlorobenzene | HCID 7964 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Chlorophenyl 2-chloro-4-nitrophenyl ketone | HCID 886296 | 50% |
Reaction Steps
Repeating Example 21 in every detail except that a chlorobenzene solution of 2-chloro-4-nitrobenzoic acid was employed in lieu of the benzene solution of the same, there is obtained a 50% yield of 2,4'-dichloro-4-nitrobenzophenone in good yield and purity having a melting point of 117° - 117.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988300 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-596521e18626411fac269b32946eda6e |
| Source note | uspto-grants-1976_10 |