HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diboron → HCID 53986416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diboron | HCID 6328200 | — |
| Reactant | 2,3-Diiodobenzoic acid | HCID 21964731 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53986416 | HCID 53986416 | — |
Reaction Steps
2,3-Diiodobenzoic acid is treated with diborane in tetrahydrofuran to give 2,3-diiodobenzyl alcohol which is oxidized to 2,3-diiodobenzaldehyde with activated manganese dioxide in methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988339 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-6ab2ca1505a54effa09106096ae5d631 |
| Source note | uspto-grants-1976_10 |