HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 54430515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 23280288 | HCID 23280288 | — |
| Reactant | HCID 54280522 | HCID 54280522 | — |
| Product | HCID 54430515 | HCID 54430515 | 93% |
Reaction Steps
The same procedure as in Example A-1 was repeated except that 2.18 g of diethyl 2,5-hexadienephosphonate and 1.42g of methyl iodide were used instead of 1.92 g of the diethyl 2-butenephosphonate and 1.7 g of the benzyl bromide respectively. Vacuum distillation of the reaction mixture afforded 2.15 g of diethyl 1-methyl-2,5-hexadienephosphonate having a boiling point of 102° C. (3 mmHg) in yield of 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988380 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-0e3dbd4d0f5443bc9d760e48cb219722 |
| Source note | uspto-grants-1976_10 |