Ethyl formate → N-[2-(4-Bromophenethyl)-phenethyl]-formamide

HRID 1288547Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1288547
[Br:1][C:2]1[CH:18]=[CH:17][C:5]([CH2:6][CH2:7][C:8]2[CH:16]=[CH:15][CH:14]=[CH:13][C:9]=2[CH2:10][CH2:11][NH2:12])=[CH:4][CH:3]=1.[CH:19](OCC)=[O:20]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][CH2:7][C:8]2[CH:16]=[CH:15][CH:14]=[CH:13][C:9]=2[CH2:10][CH2:11][NH:12][CH:19]=[O:20])=[CH:17][CH:18]=1

Komponenten

3

Edukt 2

HCID 8025Ethyl formateHCID 215028722-(4-Bromophenethyl)-phenethylamine

Produkt 1

HCID 21502878N-[2-(4-Bromophenethyl)-phenethyl]-formamide

Versuchsvorschrift

A solution of 0.60 g. (0.00197 mole) of 2-(4-bromophenethyl)-phenethylamine in 20 ml. of ethyl formate is heated to refluxing for about 19 hours. The solution is evaporated to dryness under reduced pressure and the residue dissolved in dry benzene. Evaporation of the solvent under reduced pressure leaves the product as the residual yellow oil.

Aufarbeitung

  1. temperatureto refluxing for about 19 hours
  2. customThe solution is evaporated to dryness under reduced pressure
  3. dissolutionthe residue dissolved in dry benzene
  4. customEvaporation of the solvent under reduced pressure
  5. customleaves the product as the residual yellow oil

Quellen und Nachweise

ORD-Eintrag
ord-ccdf027adc2643048b1178f27d10e492
Quelldatensatz
uspto-grants-1976_10
Patentnummer
US03988454

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