HRID1288547

反应详情

EQUATION

反应方程式

HRID 1288547 的结构方程式

PROCEDURE

实验过程

A solution of 0.60 g. (0.00197 mole) of 2-(4-bromophenethyl)-phenethylamine in 20 ml. of ethyl formate is heated to refluxing for about 19 hours. The solution is evaporated to dryness under reduced pressure and the residue dissolved in dry benzene. Evaporation of the solvent under reduced pressure leaves the product as the residual yellow oil.

WORKUP

后处理

  1. temperatureto refluxing for about 19 hours
  2. customThe solution is evaporated to dryness under reduced pressure
  3. dissolutionthe residue dissolved in dry benzene
  4. customEvaporation of the solvent under reduced pressure
  5. customleaves the product as the residual yellow oil