HRID1288547
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A solution of 0.60 g. (0.00197 mole) of 2-(4-bromophenethyl)-phenethylamine in 20 ml. of ethyl formate is heated to refluxing for about 19 hours. The solution is evaporated to dryness under reduced pressure and the residue dissolved in dry benzene. Evaporation of the solvent under reduced pressure leaves the product as the residual yellow oil.
WORKUP
后处理
- temperatureto refluxing for about 19 hours
- customThe solution is evaporated to dryness under reduced pressure
- dissolutionthe residue dissolved in dry benzene
- customEvaporation of the solvent under reduced pressure
- customleaves the product as the residual yellow oil