化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl formate → N-[2-(4-Bromophenethyl)-phenethyl]-formamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl formate | HCID 8025 | — |
| 反応物 | 2-(4-Bromophenethyl)-phenethylamine | HCID 21502872 | — |
| 生成物 | N-[2-(4-Bromophenethyl)-phenethyl]-formamide | HCID 21502878 | — |
反応手順
A solution of 0.60 g. (0.00197 mole) of 2-(4-bromophenethyl)-phenethylamine in 20 ml. of ethyl formate is heated to refluxing for about 19 hours. The solution is evaporated to dryness under reduced pressure and the residue dissolved in dry benzene. Evaporation of the solvent under reduced pressure leaves the product as the residual yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03988454 |
| 出典データセット | uspto-grants-1976_10 |
| ORD ID | ord-ccdf027adc2643048b1178f27d10e492 |
| 出典メモ | uspto-grants-1976_10 |