HRID1288568

反应详情

EQUATION

反应方程式

HRID 1288568 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a suspension of 2.7 g. of lithium aluminum hydride in 75 ml. of dry ether is added dropwise a solution containing 5.5 g. of 6-methyl-2-naphthoic acid in 75 ml. of dry ether. The mixture is refluxed for three hours, cooled, and treated with 10% sodium hydroxide solution. The mixture is then filtered and dried to yield 6-methyl-2-naphthalenemethanol.

WORKUP

后处理

  1. additionTo a suspension of 2.7 g
  2. additioncontaining 5.5 g
  3. temperatureThe mixture is refluxed for three hours
  4. temperaturecooled
  5. filtrationThe mixture is then filtered
  6. customdried