HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2-Naphthalenemethanol, 6-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 6-Methylnaphthalene-2-carboxylic acid | HCID 816843 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Naphthalenemethanol, 6-methyl- | HCID 3015042 | — |
Reaction Steps
To a suspension of 2.7 g. of lithium aluminum hydride in 75 ml. of dry ether is added dropwise a solution containing 5.5 g. of 6-methyl-2-naphthoic acid in 75 ml. of dry ether. The mixture is refluxed for three hours, cooled, and treated with 10% sodium hydroxide solution. The mixture is then filtered and dried to yield 6-methyl-2-naphthalenemethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988457 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-27060e4ca05c4ba598d92e877bac7ce5 |
| Source note | uspto-grants-1976_10 |