HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → HCID 135840366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 52119-95-6 | HCID 3711484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 135840366 | HCID 135840366 | — |
Reaction Steps
A solution of 14.1 g (0.05 mol) 3,5-di-t-butyl-4-hydroxydithiobenzoic acid and 10.4 g (0.1 mol) styrene in 100 ml toluene was heated at reflux for about 1 hour. The reaction mixture was filtered through silica gel and evaporated under reduced pressure to give the product, m.p. 70°-72° C. Elemental analysis of the product is tabulated in Table I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988471 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-b30378a618c84c8b8e01297ab386cc63 |
| Source note | uspto-grants-1976_10 |