Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isobutylene | HCID 8255 | — |
| Reactant | 52119-95-6 | HCID 3711484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 135840357 | HCID 135840357 | — |
Reaction Steps
A solution of 14.1 g (0.05 mol) 3,5-di-t-butyl-4-hydroxydithiobenzoic acid and 5.6 g (0.1 mol) isobutylene in 20 ml toluene was placed in a glass bomb tube. The tube was sealed and heated at 110° C. for 2 hours. The tube was cooled and opened. The contents were removed and evaporated under reduced pressure to give the product as an orange solid, m.p. 128°-130° C. Elemental analysis of the product is tabulated in Table I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03988471 |
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| Source dataset | uspto-grants-1976_10 |
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| ORD ID | ord-a99932681d354114a44c1a7be5cae216 |
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| Source note | uspto-grants-1976_10 |
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