HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Tolyl isocyanate → HCID 86751574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Tolyl isocyanate | HCID 69194 | — |
| Reactant | 2-Chloro-5-(4-aminobenzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine | HCID 54404537 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86751574 | HCID 86751574 | — |
Reaction Steps
As described for Example 122, a mixture of 0.348 g of 2-chloro-5-(4-aminobenzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine and 0.175 g of o-tolylisocyanate in 15 ml of tetrahydrofuran is refluxed overnight and worked-up to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05747487 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-022ef5f5b50247609b88d5d0fa3eaad8 |
| Source note | uspto-grants-1998_05 |