HCID 18925394, compound → HCID 18925413, compound

HRID 1289079Notes

Reaction equation

HRID 1289079 reaction equation
C(OC([NH:8][C:9]1[CH:13]=[CH:12][S:11][C:10]=1[C:14]([CH3:16])=[CH2:15])=O)(C)(C)C.O1CCOCC1.[ClH:23]>C(Cl)Cl>[ClH:23].[NH2:8][C:9]1[CH:13]=[CH:12][S:11][C:10]=1[C:14]([CH3:16])=[CH2:15]

Participants

4

Reactant 2

HCID 18925394HCID 18925394, compoundHCID 204431481,4-Dioxane hydrochloride

Product 1

HCID 18925413HCID 18925413, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Conditions

Temperature
0 °C

Procedure

A solution containing 0.3 g of 3-(t-butoxycarbonylamino)-2-isopropenylthiophene in 7 ml of methylene chloride was cooled to 0° C., and 3 ml of a 4N-hydrogen chloride dioxane solution was added. The mixture obtained was used as intact for the next reaction.

Workup

  1. customThe mixture obtained
  2. customintact for the next reaction

Sources & evidence

ORD record
ord-a4adbfbf3ec14df5b4d293b8f0e16d09
Source dataset
uspto-grants-1998_05
Patent number
US05747518

Reaction notes

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