Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1289079Generated: October 30, 2026

HCID 18925394, compound → HCID 18925413, compound

https://huagongshe.com/reaction/1289079

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18925394HCID 18925394—
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
SolventDichloromethaneHCID 6344—
ProductHCID 18925413HCID 18925413—

Reaction Conditions

Temperature0 °C

Reaction Steps

A solution containing 0.3 g of 3-(t-butoxycarbonylamino)-2-isopropenylthiophene in 7 ml of methylene chloride was cooled to 0° C., and 3 ml of a 4N-hydrogen chloride dioxane solution was added. The mixture obtained was used as intact for the next reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05747518
Source datasetuspto-grants-1998_05
ORD IDord-a4adbfbf3ec14df5b4d293b8f0e16d09
Source noteuspto-grants-1998_05