Sodium Acetate → HCID 86752512, compound

Participants

Reaction Steps

The 3-(4-benzoylbenzyloxy)benzaldehyde (2.0 g, 6.3 mmol) was coupled with rhodanine (1.06 g, 8.0 mmol) in the presence of sodium acetate (1.89 g, 22 mmol) and acetic acid (75 ml) essentially as previously described to yield 1.6 grams (59.0%) of the deisred title product. mp 212.5°-213.5° C. NMR. FDMS (M+) 431.

Provenance & Evidence