HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 86752518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | HCID 21191250 | HCID 21191250 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86752518 | HCID 86752518 | 52.3% |
Reaction Steps
The 4-[4-(t-butyl)phenylthio]benzaldehyde (1.5 g, 5.5 mmol) was coupled with rhodanine (0.87 g, 6.5 mmol) in the presence of sodium acetate (1.64 g, 20 mmol) and acetic acid (80 ml) essentially as previously described to yield 1.1 grams (52.3%) of the title product. mp 211°-212° C. NMR. FDMS (M+) 385.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05747517 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-e97db10243d145989ad6f35a00f67a8b |
| Source note | uspto-grants-1998_05 |