HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 86752519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | HCID 21191250 | HCID 21191250 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86752519 | HCID 86752519 | 66.7% |
Reaction Steps
The 4-[4-(t-butyl)phenylthio]benzaldehyde (1.5 g, 5.5 mmol) was condensed with rhodanine (0.865 g, 6.5 mmol) using sodium acetate (1.64 g, 20 mmol) and acetic acid (80 ml) essentially as previously described to yield 1.4 grams (66.7%) of the title compound. mp 188.5°-189.5° C. NMR. FDMS (M+) 385.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05747517 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-f717975db28f4519b0828388a4ea2697 |
| Source note | uspto-grants-1998_05 |