HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 3-Hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Hydroxybenzoic Acid | HCID 7420 | — |
| Product | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
Reaction Steps
3-hydroxybenzoic acid (30.0 g, 0.22 mol), methanol (101 ml) and concentrated sulphuric acid (2.7 ml) were added together and heated under reflux for 4 h. The reaction mixture was allowed to cool and the methanol was removed. The crude product was dried in vacuo and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750050 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-7785aeff8eeb46f79272c3b4fd31b015 |
| Source note | uspto-grants-1998_05 |