HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23206543, compound → HCID 23206558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23206543 | HCID 23206543 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23206558 | HCID 23206558 | — |
Reaction Steps
71.6 g of 1-(2,2,2-trichloroethoxycarbonyl)-6-trifluoromethyl-1,2-dihydroquinoline-2-phosphonic acid diethyl ester is dissolved in 800 ml of ethanol, mixed with 3.6 g of platinum(IV)-oxide and hydrogenated at normal pressure. It is filtered, concentrated by evaporation and recrystallized from isopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750526 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-641795bc3bb9400f89618ea2237aa057 |
| Source note | uspto-grants-1998_05 |