HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23206536, compound → HCID 23206542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23206536 | HCID 23206536 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 23206542 | HCID 23206542 | 52.2% |
Reaction Steps
6.66 g of 6-trifluoromethyl-quinoline-3-phosphonic acid diethyl ester is dissolved in 70 ml of glacial acetic acid and hydrogenated on platinum dioxide at room temperature under normal pressure. After column chromatography, 3.52 g of 6-trifluoromethyl-1,2,3,4-tetrahydroquinoline-3-phosphonic acid diethyl ester of melting point 112° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750526 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-a86a790e0855438498c4143e46d7b22d |
| Source note | uspto-grants-1998_05 |